![]() This is done by analysing parameters obtained using profile analysis of SAD (PASAD). This is not possible using X-ray, but in the TEM quanitative analysis can be obtained from an electron diffraction pattern (SAD) taken from the area of interest. On grain and domain size or on the order parameter. When studying nanocrystalline materials, it is crucial to get quantitative information on a local scale, e.g. The AutoSADP tool runs as a macro for the Digital Micrograph program and can determine d-spacing values and interplanar angles based on the pixel ratio with an accuracy of better than about 2%. The newly developed algorithm is suitable for fully automated analysis and it works well with asymmetric diffraction patterns, off-zone axis patterns, patterns with streaks, and noisy patterns such as Fast Fourier transforms of high-resolution images. The software uses iterative cross correlations to locate the forward scattered beam position and to find the coordinates of the diffraction spots. The core program, called AutoSADP, is designed to facilitate automated measurements of d-spacing and interplaner angles from TEM selected area diffraction patterns (SADPs) of single crystals. A software package 'SADP Tools' is developed as a complementary diffraction pattern analysis tool. ![]()
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